Laboratory
 
Gas-Liquid Mass Transfer
Bubble Column Hydrodynamics
X-ray Flow Visualization
Miscellaneous Equipment
 
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Dr. Ted Heindel
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Gas-Liquid Mass Transfer
Stirred Tank Reactors (3) (picture | schematic)
  • BioFlo 110 14L Fermentor (3)
    • 0 – 1200 RPM
    • Ring sparger
    • Dissolve oxygen probe
    • pH control capability
    • Temperature control capability
    • Radial flow impellers
    o Rushton (link to picture)
    o Concave (hollow) blade (link to picture)
    • Axial flow impellers
    o Philadelphia Mixing Pitched Blade Turbine (link to picture)
    o Philadelphia Mixing LS Hydrofoil (link to picture)
    o Lightnin A310 (link to picture)
    o Lightnin A315 (link to picture)
  • Dissolved carbon monoxide measurement capability
  • Extech Power Analyzer
  • Computer-controlled data acquisition system
External Loop Airlift Reactor (picture | schematic)
  • 10.2 cm ID riser
  • 2.54 cm ID downcomer
  • 2 pressure transducers
  • 2 thermocouples
  • Dissolved oxygen probe
  • 2 conductivity probes
  • Dissolved carbon monoxide measurement capability
  • 2 mass flow meters
    • 0 – 30 lpm (air)
    • 0 – 100 lpm (air)
  • Perforated plate gas distributors (1 mm diameter holes):
    • A = 0.62% (A = open area ratio)
    • A = 0.93%
    • A = 2.22%
  • Computer-controlled data acquisition system

Bubble Column Hydrodynamics
10.2 cm Semi-Batch Bubble Column (picture | schematic)
  • 2.3 m tall
  • 2 pressure transducers
  • 2 mass flow meters
    • 0 – 30 lpm (air)
    • 0 – 100 lpm (air)
  • Perforated plate gas distributors (1 mm diameter holes):
    • A = 0.62% (A = open area ratio)
    • A = 0.93%
    • A = 2.22%
  • Porous plate gas distributors:
    • 25.7% porosity (made from 0.5 micron particles)
    • 45.7% porosity (made from 20 microns particles)
    • 57.3% porosity (made from 100 microns particles)
  • Computer-controlled data acquisition system
15.2 cm Semi-Batch Bubble Column (picture | schematic)
  • 4 m tall
  • 3 pressure transducers
  • 2 thermocouples
  • 3 mass flow meters
    • 0 – 15 lpm (air)
    • 0 – 50 lpm (air)
    • 0 – 200 lpm (air)
  • Perforated plate gas distributors (1 mm diameter holes) (link to picture):
    • A = 0.57% (A = open area ratio)
    • A = 0.99%
    • A = 2.14%
  • Computer-controlled data acquisition system
32.1 cm Semi-Batch Bubble Column (picture | schematic)
  • 5.75 m tall
  • 11 pressure transducers
  • 2 thermocouples
  • 3 mass flow meters
    • 0 – 200 lpm (air)
    • 0 – 500 lpm (air)
    • 0 – 1000 lpm (air)
  • Perforated plate gas distributors (1 mm diameter holes)
    • A = 0.49% (A = open area ratio) (link to picture)
    • A = 0.95% (link to picture)
    • A = 2.03% (link to picture)
  • Computer-controlled data acquisition system
15.2 cm Cocurrent Bubble Column (picture | schematic)
  • 4 m tall
  • 5 pressure transducers
  • 2 thermocouples
  • 3 mass flow meters
    • 0 – 30 lpm (air)
    • 0 – 100 lpm (air)
    • 0 – 500 lpm (air)
  • Magnetic flow meter
    • 0-195 lpm (water)
  • 100 gal storage tank
  • 7.5 hp slurry pump with variable frequency drive
  • 0.5 hp mixer
  • Radial gas distributor (link to picture | link to schematic)
  • Computer-controlled data acquisition system

X-ray Flow Visualization (link to picture | link to schematic)
LORAD LPX200 portable X-ray unit (2) (picture)
  • 10-200 kV, 0.1-10 mA, 900 W (max)
  • 1.5 mm spot size
  • 60° horizontal, 40° vertical cone beam
Precise Optics PS164X image intensifier (2) (picture)
  • Input region: 40.6 cm diameter
  • Output region: 35 mm diameter
DVC-1412 CCD camera (2)
  • Pixel size: 6.45 µm x 6.45 µm
  • Active pixels: 1388(H) x 1024(V)
  • Frame rate (binning): 10 fps (1x1), 20 fps (2x2), 40 fps (4x4), 60 fps (8x8)
Motorized zoom lens (2)
  • 12.5-75 mm
Hamamatsu CsI phosphor screen (link to picture when available)
  • Input region: 44 cm x 44 cm (square)
Apogee Alta U9 CCD camera
  • Pixel size: 9 µm x 9 µm
  • Active pixels: 3072(H) x 2048(V)
  • Thermoelectric cooler for low noise and long exposures
  • Digitized signal capability of either 12 bit or 16 bit
Rotation system (picture)
  • Rotek 101.4 cm ID 150 tooth slewing ring
  • 30 tooth pinion gear
  • Parker 25:1 gearbox
  • Compumotor stepper motor and ZETA6112 controller
Vertical lift system (picture)
  • 910 kg (2000 lb) winch
  • Vertical track with 2.75 m travel
  • Approximately 4 m span in imaging region (with table extensions)
Control and data acquisition computer
  • 3.0 GHz Pentium processor
  • 250 GB hard-drive (2)
  • 4 GB PC3200 DDR RAM
  • Custom software for image acquisition, reconstruction, and visualization
Image reconstruction computer
  • 64-node LINUX cluster

Miscellaneous Equipment
  • Ventilated gas cylinder cabinet (picture)
  • Black Clawson Hydrapulper (picture)
  • British disintegrator (picture)
  • Sigma 703 surface tension analyzer (picture)
  • Milwaukee pH/EC/TDS meter (link to picture when available)
  • Stir-Pak laboratory mixer, 23-2300 RPM (2) (picture)
  • DiskFlo 7.5 hp centrifugal pump (picture)